sodium hydride
1.) THF, 0.5 h, 2.) reflux, 6 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brownbridge, Peter; Hunt, Paul G.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1695 - 1706
ammonium chloride; zinc in water
1 h; various propargyl halides, acidic salt solutions or basic medium; various rate of products; Product distribution;
参考文献
Bieber, Lothar W.; Da Silva, Margarete F.; Da Costa, Rosenildo C.; Silva, Lilia O.S.
Tetrahedron Letters, 1998 , vol. 39, # 22 p. 3655 - 3658
in tetrachloromethane
T=35 - 40°C; 18 h; Irradiation;
参考文献
Drozdova, T. I.; Kozyreva, O. B.; Levkovskaya, G. G.; Mirskova, A. N.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 3.1 p. 409 - 412
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 3 p. 381 - 384