3,3-二甲基-1-丁基酸酯合成路线 （共 65 条）
反应条件
T=300°C; P=73550.8 Torr;
参考文献
Pines et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5099,5101
反应条件
T=220°C; P=73550.8 Torr; Produkt5: Aethan;
参考文献
Ipatieff et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 553
反应条件
T=400°C; und Hydrieren des Reaktionsprodukts an Nickel/Kieselgur bei 70grad/70 at;
参考文献
Ipatieff et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 553
反应条件
potassium hydroxide; oxygen in ethylene glycol dimethyl ether T=20°C; 14 h;
参考文献
Artamkina, G.A.; Grinfel'd, A.A.; Beletskaya, I.P.
Tetrahedron Letters, 1984 , vol. 25, # 43 p. 4989 - 4992
反应条件
copper(II) oxide T=300°C; Gas phase;
参考文献
The NutraSweet Company
Patent: EP1186591 A2, 2002 ;
Location in patent: Page column 3 ;
反应条件
hydrogenchloride; zinc(II) chloride
参考文献
Lee, Sueg-Geun
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 7 p. 1361 - 1372
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 5 h;
参考文献
Hen, Naama; Bialer, Meir; Yagen, Boris
Journal of Medicinal Chemistry, 2012 , vol. 55, # 6 p. 2835 - 2845
反应条件
(i) Py, (ii) liq. NH3; Multistep reaction;
参考文献
Fessenden; Coon
Journal of medicinal chemistry, 1965 , vol. 8, # 5 p. 604 - 608
反应条件
1.1: 99.2 percent / PBr3; pyridine / 12 h / Heating 2.1: Mg / diethyl ether / 2 h / 20 °C 2.2: 43.9 percent / diethyl ether / 1 h / 20 °C 3.1: 44.8 percent / LiAlH4 / diethyl ether / 5 h / Heating View Scheme
参考文献
Hamano, Hiroshi; Nagata, Keiichi; Fukada, Nobuo; Shimotahira, Hiroshi; Ju, Xiu-Lian; Ozoe, Yoshihisa
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 3 p. 665 - 674
反应条件
1.1: 99.2 percent / PBr3; pyridine / 12 h / Heating 2.1: Mg / diethyl ether / 2 h / 20 °C 2.2: 43.9 percent / diethyl ether / 1 h / 20 °C View Scheme
参考文献
Lee, Sueg-Geun
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 7 p. 1361 - 1372
