1-(2-溴苯基)丙烷-1-酮合成路线 （共 12 条）
参考文献
Basell Polypropylen GmbH
Patent: US6492539 B1, 2002 ;
反应条件
in N,N-dimethyl-formamide
参考文献
Boehringer Ingelheim Pharma KG
Patent: US6043254 A1, 2000 ;
US 6043254 A
反应条件
silica gel; pyridinium chlorochromate in dichloromethane
T=20°C; 2 h; Inert atmosphere;
参考文献
Mahendar, Lodi; Krishna, Jonnada; Gopi Krishna Reddy, Alavala; Venkat Ramulu, Bokka; Satyanarayana, Gedu
Organic Letters, 2012 , vol. 14, # 2 p. 628 - 631
反应条件
bromine in dichloromethane
参考文献
Bayer Aktiengesellschaft
Patent: US4578396 A1, 1986 ;
反应条件
1: tetrahydrofuran / 3.5 h / -78 - 25 °C
2: H2CrO4 / diethyl ether / 3 h / 25 °C
View Scheme
参考文献
Boger, Dale L.; Duff, Steven R.; Panek, James S.; Yasuda, Masami
Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5782 - 5789
反应条件
in tetrahydrofuran; diethyl ether
4 h; Ambient temperature;
参考文献
Wang, Shaopeng; Morrow, Gary W.; Swenton, John S.
Journal of Organic Chemistry, 1989 , vol. 54, # 22 p. 5364 - 5371
反应条件
in hexane; toluene
2 h; Ambient temperature;
参考文献
Morrow, Gary W.; Chen, Ying; Swenton, John S.
Tetrahedron, 1991 , vol. 47, # 415 p. 655 - 664
反应条件
1: SOCl2, DMF / Heating
2: 89 percent / tetrahydrofuran; diethyl ether / 4 h / Ambient temperature
View Scheme
参考文献
Wang, Shaopeng; Morrow, Gary W.; Swenton, John S.
Journal of Organic Chemistry, 1989 , vol. 54, # 22 p. 5364 - 5371
反应条件
hydrogen bromide; copper(I) bromide
参考文献
Elson; Gibson; Johnson
Journal of the Chemical Society, 1930 , p. 1128,1131
Full Text Show Details
Zenitz; Hartung
Journal of Organic Chemistry, 1946 , vol. 11, p. 444,447
反应条件
diethyl ether; ethylmagnesium bromide
anschliessendes Behandeln mit Eis und wss. HCl;
参考文献
Borsche; Scriba
Justus Liebigs Annalen der Chemie, 1939 , vol. 541, p. 283,290
