3-呋喃核糖基-1,2,4-三唑-5-甲酰胺合成路线 (共 7 条)
反应条件
T=135°C; P=0.1 Torr; 0.25 h;
参考文献
Poonian; Nowoswiat
Journal of Organic Chemistry, 1980 , vol. 45, # 2 p. 203 - 208
参考文献
Vanek,T. et al.
Collection of Czechoslovak Chemical Communications, 1979 , vol. 44, p. 1334 - 1338
反应条件
1: 2-methoxy-ethanol
2: NaOMe / methanol
3: NH3 / methanol
View Scheme
参考文献
Vanek,T. et al.
Collection of Czechoslovak Chemical Communications, 1979 , vol. 44, p. 1334 - 1338
参考文献
Vanek,T. et al.
Collection of Czechoslovak Chemical Communications, 1979 , vol. 44, p. 1334 - 1338
参考文献
Huynh-Dinh; Igolen; Bisagni; Marquet; Civier
Journal of the Chemical Society. Perkin transactions 1, 1977 , # 7 p. 761 - 764
反应条件
1: 71.3 percent / dimethylsulfoxide / 20 h / Ambient temperature
2: 62.2 percent / 0.25 h / 135 °C / 0.1 Torr
View Scheme
参考文献
Poonian; Nowoswiat
Journal of Organic Chemistry, 1980 , vol. 45, # 2 p. 203 - 208
反应条件
1: 70 percent / methanol / 2.5 h / Ambient temperature
2: 71.3 percent / dimethylsulfoxide / 20 h / Ambient temperature
3: 62.2 percent / 0.25 h / 135 °C / 0.1 Torr
View Scheme
参考文献
Poonian; Nowoswiat
Journal of Organic Chemistry, 1980 , vol. 45, # 2 p. 203 - 208