三乙基(1,4-戊二烯-3-基氧基)硅烷合成路线 （共 17 条）
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile T=150°C; 0.05 h; Microwave irradiation;
参考文献
Journal of Organic Chemistry, , vol. 74, # 5 p. 2179 - 2182
反应条件
1H-imidazole in N,N-dimethyl-formamide
T=25°C; 15 h;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
1: sec-BuLi / tetrahydrofuran; cyclohexane / -78 °C
2: 78 percent / KF / methanol / 3 h / -5 °C
View Scheme
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
(i) sBuLi, THF, (ii) /BRN= 4977102/; Multistep reaction;
参考文献
Oppolzer,W.; Snowden,R.L.
Tetrahedron Letters, 1976 , p. 4187 - 4190
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
(i) sBuLi, THF, (ii) /BRN= 605308/; Multistep reaction;
参考文献
Oppolzer,W.; Snowden,R.L.
Tetrahedron Letters, 1976 , p. 4187 - 4190
