三乙基(1,4-戊二烯-3-基氧基)硅烷合成路线 （共 17 条）
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
potassium fluoride; sec.-butyllithium
1.) THF/cyclohexane, -78 deg C; 2.) from 0 deg C to 15 deg C, 15 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
(i) sBuLi, THF, (ii) /BRN= 385801/; Multistep reaction;
参考文献
Oppolzer,W.; Snowden,R.L.
Tetrahedron Letters, 1976 , p. 4187 - 4190
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
(i) sBuLi, THF, (ii) /BRN= 102378/; Multistep reaction;
参考文献
Oppolzer,W.; Snowden,R.L.
Tetrahedron Letters, 1976 , p. 4187 - 4190
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
反应条件
1: sec-BuLi / tetrahydrofuran; cyclohexane / -78 °C
2: 84 percent / toluene / 17 h / 160 °C
View Scheme
参考文献
Oppolzer, Wolfgang; Snowden, Roger L.; Simmons, Dana P.
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2002 - 2021
