4-(癸基氧基)苯甲酸甲酯合成路线 （共 13 条）
参考文献
Bhattacharya, Santanu; Subramanian, Marappan; Hiremath, Uma S.
Chemistry and Physics of Lipids, 1995 , vol. 78, # 2 p. 177 - 188
参考文献
Hegmann, Torsten; Marx, Vanessa M.
Patent: US2011/62385 A1, 2011 ;
反应条件
1: aq. KOH / methanol / 12 h / Heating 2: DCC, DMAP / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
1: methyl 4-hydroxy-benzoate With potassium carbonate in acetonitrile
T=70°C; Inert atmosphere;
2: 1-bromo-decane in acetonitrile
12 h; RefluxInert atmosphere;
参考文献
Marx, Vanessa M.; Girgis, Hidy; Heiney, Paul A.; Hegmann, Torsten
Journal of Materials Chemistry, 2008 , vol. 18, # 25 p. 2983 - 2994
反应条件
sodium methylate in N,N-dimethyl-formamide
参考文献
Parker,R.A. et al.
Journal of Medicinal Chemistry, 1977 , vol. 20, p. 781 - 791
反应条件
sulfuric acid
Heating;
参考文献
Cohen, Yael; Bodner, Efrat; Richman, Michal; Afri, Michal; Frimer, Aryeh A.
Chemistry and Physics of Lipids, 2008 , vol. 155, # 2 p. 98 - 113
反应条件
1: potassium hydroxide / ethanol; water / 2 h / |Reflux
2: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / |Reflux
3: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
4: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
反应条件
1: aq. KOH / methanol / 12 h / Heating
2: DCC, DMAP / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
1: aq. KOH / methanol / 12 h / Heating
2: DCC, DMAP / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
1: aq. NaOH / methanol / Heating
2: SOCl2 / Heating
View Scheme
参考文献
Ili, Monica; Bucos, Madalina; Dumitracu, Florea; Circu, Viorel
Journal of Molecular Structure, 2011 , vol. 987, # 1-3 p. 1 - 6
