3-氨基-1-甲基-5H-吡啶[4,3-B]吲哚合成路线 （共 20 条）
反应条件
acetic acid in water
参考文献
Molina, Pedro; Almendros, Pedro; Fresneda, Pilar M.
Tetrahedron Letters, 1993 , vol. 34, # 29 p. 4701 - 4704
反应条件
ammonia T=100°C; 5 h;
参考文献
Akimoto, Hiroshi; Kawai, Akiyoshi; Nomura; Hiroaki
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, p. 123 - 130
反应条件
sodium hydroxide; diphenylphosphoranyl azide; acetic acid; triethylamine Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, p. 123 - 130
反应条件
1: 98 percent / LiOH / H2O; tetrahydrofuran / Ambient temperature 2: 98 percent / Ph2PON3, NEt3 3: 80 percent / HOAc / H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 29 p. 4701 - 4704
反应条件
1: ethanol / 1 h / 20 °C 3: 24 percent / phosphoryl chloride / 2 h / 85 °C 4: 58 percent / 20percent methanolic ammonia / 5 h / 100 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, p. 123 - 130
反应条件
2: 24 percent / phosphoryl chloride / 2 h / 85 °C 3: 58 percent / 20percent methanolic ammonia / 5 h / 100 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, p. 123 - 130
反应条件
1: 53 percent / t-BuLi / diethyl ether 2: 70 percent / NaOEt / ethanol / -15 °C 3: 85 percent / CH2Cl2 / Ambient temperature 4: 85 percent / toluene / 12 h / 160 °C 5: 70 percent / HCOOH / Heating 6: 98 percent / LiOH / H2O; tetrahydrofuran / Ambient temperature 7: 98 percent / Ph2PON3, NEt3 8: 80 percent / HOAc / H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 29 p. 4701 - 4704
反应条件
1: 70 percent / NaOEt / ethanol / -15 °C 2: 85 percent / CH2Cl2 / Ambient temperature 3: 85 percent / toluene / 12 h / 160 °C 4: 70 percent / HCOOH / Heating 5: 98 percent / LiOH / H2O; tetrahydrofuran / Ambient temperature 6: 98 percent / Ph2PON3, NEt3 7: 80 percent / HOAc / H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 29 p. 4701 - 4704
反应条件
1: 85 percent / CH2Cl2 / Ambient temperature 2: 85 percent / toluene / 12 h / 160 °C 3: 70 percent / HCOOH / Heating 4: 98 percent / LiOH / H2O; tetrahydrofuran / Ambient temperature 5: 98 percent / Ph2PON3, NEt3 6: 80 percent / HOAc / H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 29 p. 4701 - 4704
反应条件
1: 70 percent / HCOOH / Heating 2: 98 percent / LiOH / H2O; tetrahydrofuran / Ambient temperature 3: 98 percent / Ph2PON3, NEt3 4: 80 percent / HOAc / H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 29 p. 4701 - 4704
