4,5-二乙基吡咯[1,2-a]喹啉合成路线 （共 2 条）
反应条件
1: 1-phenyl-1H-pyrrole With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in hexane
T=-78°C;
2: With anhydrous chromium(III) chloride in tetrahydrofuran; hexane
T=20°C; 1 h;
3: hex-3-yne in tetrahydrofuran; hexane
T=50°C; 12 h;
参考文献
Kanno, Ken-Ichiro; Liu, Yuanhong; Iesato, Atsushi; Nakajima, Kiyohiko; Takahashi, Tamotsu
Organic Letters, 2005 , vol. 7, # 24 p. 5453 - 5456
反应条件
copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide
T=160°C; 48 h; Inert atmosphere; regioselective reaction;
参考文献
Liao, Qian; Zhang, Liyun; Li, Shutao; Xi, Chanjuan
Organic Letters, 2011 , vol. 13, # 2 p. 228 - 231
