lithium salt of 2-nitropropane in N,N,N',N',N'',N''-hexamethylphosphoric triamide 5 h; Ambient temperatureIrradiation;

1: 1.) t-BuOK / 1.) Me2SO, room temp., 2.) Me2SO, irradiation, room temp., 6 h 2: 74 percent / lithium salt of 2-nitropropane / hexamethylphosphoric acid triamide / 5 h / Ambient temperature; Irradiation View Scheme

N,N,N',N',N'',N''-hexamethylphosphoric triamide Irradiation;

Yield given. Multistep reaction;