2,4-二羟基-3-甲基苯甲醛合成路线 (共 15 条)
反应条件
hydrogenchloride in diethyl ether T=20°C;
参考文献
Cook, Silas P.; Polara, Alessandra; Danishefsky, Samuel J.
Journal of the American Chemical Society, 2006 , vol. 128, # 51 p. 16440 - 16441
反应条件
trichlorophosphate T=20°C; 12 h;
参考文献
Moreau, Anne; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre; Lebrun, Stephane
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 12 p. 2305 - 2309
反应条件
trichlorophosphate in water; acetone
参考文献
E. I. Du Pont de Nemours and Company
Patent: US5102785 A1, 1992 ;
反应条件
1: With hydrogenchloride; potassium chloride in diethyl ether Gattermann aldehyde synthesis; 2: With water in diethyl ether Gattermann aldehyde synthesis;
参考文献
Journal of Heterocyclic Chemistry, , vol. 47, # 3 p. 729 - 733
反应条件
hydrogenchloride; water 1.) ether; 2.) ether, heating; Yield given. Multistep reaction;
参考文献
Phytochemistry (Elsevier), , vol. 28, # 1 p. 239 - 242
反应条件
1: aqueous HI 2: diethyl ether / Einleiten von HCl und Erhitzen des Reaktionsprodukts mit Wasser View Scheme
参考文献
Journal of the Chemical Society, , p. 1689,1691
反应条件
potassium cyanide; manganese(IV) oxide in acetic acid T=20°C; Oxidation; esterification;
参考文献
Peixoto, Christophe; Laurin, Patrick; Klich, Michel; Dupuis-Hamelin, Claudine; Mauvais, Pascale; Lassaigne, Patrice; Bonnefoy, Alain; Musicki, Branislav
Tetrahedron Letters, 2000 , vol. 41, # 11 p. 1741 - 1745
反应条件
potassium carbonate in acetone 5 h; Heating;
参考文献
Barber, Jill; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1685 - 1689
反应条件
phosphoric acid; palladium in ethyl acetate; isopropyl alcohol
参考文献
E. I. Du Pont de Nemours and Company
Patent: US5102785 A1, 1992 ;