(3-羧丙基)三甲基氯化铵合成路线 （共 8 条）
反应条件
hydrogenchloride in water T=20°C;
参考文献
Gasparini, Giulio; Prins, Leonard J.; Scrimin, Paolo
Angewandte Chemie - International Edition, 2008 , vol. 47, # 13 p. 2475 - 2479
反应条件
1: [14C]-4-Aminobutyric acid With potassium hydrogencarbonate in methanol 0.25 h; Inert atmosphere; 2: methyl iodide in methanol T=20°C; 66 h; Inert atmosphere; 3: With hydrogenchloride in water
参考文献
Morano, Cain; Zhang, Xin; Fricker, Lloyd D.
Analytical Chemistry, 2008 , vol. 80, # 23 p. 9298 - 9309
反应条件
1: in acetone T=20°C; 72 h; 2: With hydrogenchloride; water
参考文献
Beierlein, Christian H.; Breit, Bernhard; Paz Schmidt, Roberto A.; Plattner, Dietmar A.
Organometallics, 2010 , vol. 29, # 11 p. 2521 - 2532
反应条件
1: conc. HCl / 10 h 2: 1.) formic acid, 2.) HCl / H2O / 1.) reflux, 7h, 2.) reflux, 1.5h 3: NaOH aq. / ethanol / 0 °C / overnight 4: 2.) conc. HCl / 1.) MeOH, 48h, then 50 deg C, 3h View Scheme
参考文献
Synthesis, , # 6 p. 468 - 469
反应条件
1: NaOH aq. / ethanol / 0 °C / overnight 2: 2.) conc. HCl / 1.) MeOH, 48h, then 50 deg C, 3h View Scheme
参考文献
Synthesis, , # 6 p. 468 - 469
反应条件
hydrogenchloride 1.) H2O, acetone, 3d; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 55, # 4 p. 1334 - 1338
反应条件
hydrogenchloride 1.) MeOH, 48h, then 50 deg C, 3h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 6 p. 468 - 469
参考文献
Journal of Molecular Structure, , vol. 563-564, p. 555 - 564
