potassium naphthalenide in tetrahydrofuran
T=-40°C;
参考文献
Bhandari, Prabha; Crombie, Leslie; Harper, Mark F.; Rossiter, John T.; Sanders, Mark; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1685 - 1698
1: CH2Cl2 / 1 h / -10 °C
2: sodium borohydride / bis-(2-methoxy-ethyl) ether / 0.5 h / 0 °C
3: 55 percent / potassium naphthalenide / tetrahydrofuran / -40 °C
View Scheme
参考文献
Bhandari, Prabha; Crombie, Leslie; Harper, Mark F.; Rossiter, John T.; Sanders, Mark; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1685 - 1698
1: 88 percent / 1,2-dichlorobenzene / 24 h / Heating
2: CH2Cl2 / 1 h / -10 °C
3: sodium borohydride / bis-(2-methoxy-ethyl) ether / 0.5 h / 0 °C
4: 55 percent / potassium naphthalenide / tetrahydrofuran / -40 °C
View Scheme
参考文献
Bhandari, Prabha; Crombie, Leslie; Harper, Mark F.; Rossiter, John T.; Sanders, Mark; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1685 - 1698
1: sodium borohydride / bis-(2-methoxy-ethyl) ether / 0.5 h / 0 °C
2: 55 percent / potassium naphthalenide / tetrahydrofuran / -40 °C
View Scheme
参考文献
Bhandari, Prabha; Crombie, Leslie; Harper, Mark F.; Rossiter, John T.; Sanders, Mark; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1685 - 1698
