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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-氨基戊烷
合成路线
（共 28 条）
64-17-5
乙醇
+
625-30-9
2-氨基戊烷
→
反应条件
1817-89-6
2-乙氧基戊烷
反应条件
7-phenyl-5,6,8,9-tetrahydrodibenzolt;c,hgt;xanthylium trifluoromethanesulphonate; triethylamine T=25°C; 96 h;
参考文献
Katritzky, Alan R.; Lopez-Rodriguez, Maria L.; Keay, James G.; King, Roy W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 165 - 170
127-17-3
丙酮酸
+
625-30-9
2-氨基戊烷
→
反应条件
56-41-7
氨基丙酸
+
107-87-9
2-戊酮
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. phosphate buffer T=37°C; pH=7.4; 0.0833333 h; Enzymatic reaction; enantioselective reaction;
参考文献
Jiang, Jinju; Chen, Xi; Feng, Jinhui; Wu, Qiaqing; Zhu, Dunming
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 32 - 39
625-30-9
2-氨基戊烷
→
反应条件
625-30-9
2-氨基戊烷
+
107-87-9
2-戊酮
反应条件
transaminase ATA-114; pyridoxal 5'-phosphate; sodium 2-oxopropanoate T=30°C; pH=7.0; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Koszelewski, Dominik; Clay, Dorina; Rozzell, David; Kroutil, Wolfgang
European Journal of Organic Chemistry, 2009 , # 14 p. 2289 - 2292
625-30-9
2-氨基戊烷
→
反应条件
107-87-9
2-戊酮
+
54542-13-1
反应条件
transaminase ATA-117; pyridoxal 5'-phosphate; sodium 2-oxopropanoate T=30°C; pH=7.0; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Koszelewski, Dominik; Clay, Dorina; Rozzell, David; Kroutil, Wolfgang
European Journal of Organic Chemistry, 2009 , # 14 p. 2289 - 2292
625-30-9
2-氨基戊烷
→
反应条件
625-30-9
2-氨基戊烷
+
107-87-9
2-戊酮
+
54542-13-1
反应条件
transaminase ATA-113; pyridoxal 5'-phosphate; sodium 2-oxopropanoate T=30°C; pH=7.0; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Koszelewski, Dominik; Clay, Dorina; Rozzell, David; Kroutil, Wolfgang
European Journal of Organic Chemistry, 2009 , # 14 p. 2289 - 2292
72-19-5
L-苏氨酸
+
625-30-9
2-氨基戊烷
→
反应条件
1492-24-6
L-2-氨基丁酸
+
625-30-9
2-氨基戊烷
+
107-87-9
2-戊酮
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 9 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
127-17-3
丙酮酸
+
625-30-9
2-氨基戊烷
→
反应条件
56-41-7
氨基丙酸
+
107-87-9
2-戊酮
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. phosphate buffer T=37°C; pH=7.4; 0.0833333 h; Enzymatic reaction; enantioselective reaction;
参考文献
Jiang, Jinju; Chen, Xi; Feng, Jinhui; Wu, Qiaqing; Zhu, Dunming
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 32 - 39
591-50-4
碘苯
+
625-30-9
2-氨基戊烷
→
反应条件
2716-62-3
反应条件
potassium carbonate in N,N-dimethyl-formamide T=25°C; 10 h; Inert atmosphere;
参考文献
Arundhathi, Racha; Kumar, Desitti Chaitanya; Sreedhar, Bojja
European Journal of Organic Chemistry, 2010 , # 19 p. 3621 - 3630
625-30-9
2-氨基戊烷
→
反应条件
2084-19-7
2-戊硫醇
反应条件
hydrogen sulfide T=300°C; P=75.006 Torr; Kinetics; Further Variations:PressuresTemperatures;
参考文献
Zhao; Prins
Journal of Catalysis, 2004 , vol. 222, # 2 p. 532 - 544
625-30-9
2-氨基戊烷
→
反应条件
625-30-9
2-氨基戊烷
+
107-87-9
2-戊酮
反应条件
transaminase ATA-114; pyridoxal 5'-phosphate; sodium 2-oxopropanoate T=30°C; pH=7.0; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Koszelewski, Dominik; Clay, Dorina; Rozzell, David; Kroutil, Wolfgang
European Journal of Organic Chemistry, 2009 , # 14 p. 2289 - 2292
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