反应条件
1.1: Br2; potassium acetate / methanol / 1 h / 0 °C
1.2: 35 percent / aq. HBr / methanol / 20 °C
2.1: 94 percent / benzene / 1 h / Heating
3.1: 96 percent / H2 / Pd/C / methanol
4.1: 91 percent / lithium aluminum hydride / diethyl ether / 20 °C
5.1: 93 percent / pyridine / 3 h / -10 °C
6.1: 80 percent / potassium tert-butylate; dimethyl sulfoxide / 40 °C
7.1: potassium tert-butoxide; DMSO / 4 h / 60 °C
View Scheme
参考文献
Lee, Patrick S.; Sakai, Shogo; Hoerstermann, Peter; Roth, Wolfgang R.; Kallel, E. Adam; Houk
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5839 - 5848
