(R)-2-(羟基甲基)-1,4-苯并二噁烷合成路线 （共 33 条）
反应条件
lipase PS immobilized on Toyonite with MeCO2(CH2)6Si(OMe)3 in dichloromethane T=0°C; Enzymatic reaction; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 76, # 7 p. 1441 - 1446
反应条件
1: pyridine / 0 °C
2: dimethylformamide / Heating
3: NH2-NH2*H2O / 2-methoxy-ethanol / Heating
View Scheme
参考文献
Ferri; Pallavicini; Piccini; Valoti; Villa
Farmaco, Edizione Scientifica, 1988 , vol. 43, # 12 SUPPL. p. 1153 - 1163
反应条件
1: potassium hydroxide; potassium permanganate / water; acetone / 0.5 h / 0 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / tetrahydrofuran; dichloromethane / 0 °C
3: trifluoroacetic acid / dichloromethane / 1 h / 0 °C
View Scheme
参考文献
Rouf, Abdul; Aga, Mushtaq A.; Kumar, Brijesh; Taneja, Subhash Chandra
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6420 - 6422
