8-溴-6-甲基-3,4-二氢-2H-1,4-苯并恶嗪合成路线 （共 3 条）
反应条件
dimethylsulfide borane complex in tetrahydrofuran
Heating;
参考文献
Zhao, Shu-Hai; Berger, Jacob; Clark, Robin D.; Sethofer, Steven G.; Krauss, Nancy E.; Brothers, Julie M.; Martin, Renee S.; Misner, Dinah L.; Schwab, Dietmar; Alexandrova, Ludmila
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3504 - 3507
反应条件
1: 68 percent / Na2S2O4 / ethanol; H2O / 70 °C
2: 95 percent / Na2CO3 / acetonitrile; H2O / 10 h / 60 °C
3: 89 percent / BH3-DMS / tetrahydrofuran / Heating
View Scheme
参考文献
Zhao, Shu-Hai; Berger, Jacob; Clark, Robin D.; Sethofer, Steven G.; Krauss, Nancy E.; Brothers, Julie M.; Martin, Renee S.; Misner, Dinah L.; Schwab, Dietmar; Alexandrova, Ludmila
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3504 - 3507
反应条件
1: 95 percent / Na2CO3 / acetonitrile; H2O / 10 h / 60 °C
2: 89 percent / BH3-DMS / tetrahydrofuran / Heating
View Scheme
参考文献
Zhao, Shu-Hai; Berger, Jacob; Clark, Robin D.; Sethofer, Steven G.; Krauss, Nancy E.; Brothers, Julie M.; Martin, Renee S.; Misner, Dinah L.; Schwab, Dietmar; Alexandrova, Ludmila
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3504 - 3507
