反应条件
1: 1,3,5-trimethyl-1H-pyrazole With n-butyllithium in tetrahydrofuran; hexane
T=-80 - 20°C; Inert atmosphere;
2: chloro-trimethyl-silane in tetrahydrofuran; hexane
T=-80 - 20°C; Inert atmosphere;
参考文献
Jin, Can; Wang, Zhong-Xia
New Journal of Chemistry, 2009 , vol. 33, # 3 p. 659 - 667