2,3,5,6-四氟硝基苯合成路线 （共 11 条）
反应条件
4-(N,N-dimethlyamino)pyridine; C21H27AuN2 in dichloromethane T=40°C; 12 h; Inert atmosphere; ConcentrationReagent/catalystSolvent;
参考文献
Lv, Hongbin; Zhan, Jin-Hui; Cai, Yuan-Bo; Yu, Yi; Wang, Bingwu; Zhang, Jun-Long
Journal of the American Chemical Society, 2012 , vol. 134, # 39 p. 16216 - 16227,12
反应条件
water; fluorine in acetonitrile T=20°C; 5 h; Inert atmosphereFlow reactor;
参考文献
McPake, Christopher B.; Murray, Christopher B.; Sandford, Graham
ChemSusChem, 2012 , vol. 5, # 2 p. 312 - 319
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide electrolysis;
参考文献
Ryabinin, V. A.; Starichenko, V. F.; Shteingarts, V. D.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 7.1 p. 1143 - 1148
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 7 p. 1379 - 1386
反应条件
t-Bu-XantPhos; tBuXantphosAu(AuCl2); (Ph)2SiH2; acetic acid in 1,2-dichloro-ethane T=80°C; 24 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 8 p. 1529 - 1541
反应条件
boron trifluoride; nitric acid; nitrogen(IV) oxide in sulfolane
参考文献
Tetrahedron, , vol. 24, p. 5913 - 5916
反应条件
nitronium tetrafluoroborate in sulfolane T=50°C; 12 h; other temperatures and reagents; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, # 4 p. 742 - 748
Zhurnal Organicheskoi Khimii, , vol. 22, # 4 p. 831 - 837
反应条件
XantphosAuCl; Xantphos; (Ph)2SiH2; trifluoroacetic acid in 1,2-dichloro-ethane T=80°C; 24 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 8 p. 1529 - 1541
反应条件
water; epoxysulfonyl fluoride 1.) 25 deg C, 1.5 h; 2.) 0 deg C; Yield given. Multistep reaction;
参考文献
Journal of Fluorine Chemistry, , vol. 22, p. 345 - 376
反应条件
sulfuric acid; water 1.) 20 deg C, 2 h; 2.) 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 22, p. 345 - 376
反应条件
ammonium chloride in N,N-dimethyl-formamide electrolysis, var. proton donors; also 1,4-dinitrobenzene and 1,4-dinitrodurene; Mechanism;
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 7.1 p. 1143 - 1148
Zhurnal Organicheskoi Khimii, , vol. 29, # 7 p. 1379 - 1386
