4,4’-双(二甲氨基)偶氮苯合成路线 （共 29 条）
反应条件
in various solvent(s)
T=155°C; 8 h;
参考文献
Nay, Barry; Scriven, Eric F. V.; Suschitzky, Hans; Thomas, Desmond R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 611 - 613
反应条件
(i) Li, (ii) /BRN= 607293/, THF; Multistep reaction;
参考文献
Antkowiak,T.A.; Shechter,H.
Journal of the American Chemical Society, 1972 , vol. 94, p. 5361 - 5366
反应条件
in tetrahydrofuran
T=-20°C; 1 h;
参考文献
Todres, Z. V.; Ovsepyan G. Ts.; Kosnikov, A. Yu.; Lindeman, S. V.; Struchkov, Yu. T.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 3.2 p. 522 - 527
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 3 p. 610 - 616
反应条件
in tetrahydrofuran
T=-20°C; 1 h;
参考文献
Todres, Z. V.; Ovsepyan G. Ts.; Kosnikov, A. Yu.; Lindeman, S. V.; Struchkov, Yu. T.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 3.2 p. 522 - 527
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 3 p. 610 - 616
反应条件
ethanol; nitrogen oxides
参考文献
Lippmann; Lange
Chemische Berichte, 1880 , vol. 13, p. 2137
Full Text Show Details
Lippmann; Fleissner
Chemische Berichte, 1882 , vol. 15, p. 2138; 16,1416
Monatshefte fuer Chemie, 1882 , vol. 3, p. 708; 4,284
反应条件
diethyl ether; ethanol
参考文献
Fischer,O.; Wacker
Chemische Berichte, 1888 , vol. 21, p. 2610
Full Text Show Details
Noelting; Fourneaux
Chemische Berichte, 1897 , vol. 30, p. 2934
参考文献
Kaplan; Haddon; Raghavachari; Menezes; Schilling; Hauser; Marshall
Molecular crystals and liquid crystals, 1982 , vol. 80, # 1-4 p. 51 - 66
参考文献
Barbier; Vignon
Bulletin de la Societe Chimique de France, 1887 , vol. <2>48, p. 637
Full Text Show Details
Noelting; Fourneaux
Chemische Berichte, 1897 , vol. 30, p. 2934
反应条件
potassium ethanolate
参考文献
Bamberger
Justus Liebigs Annalen der Chemie, 1920 , vol. 420, p. 137
参考文献
Quilico
Gazzetta Chimica Italiana, 1928 , vol. 58, p. 322
