反应条件
1: 1.) KH, triethylborane / 1.) THF, 12 h, 25 deg C; 2.) 10 h, THF
2: 1.) Me3SiCH(Li)OMe / 1.) 25 deg C, overnight; 2.) 15 min; 2 h, reflux
3: KMnO4, H2SO4
View Scheme
参考文献
Baigrie,L.M.; Seiklay,H.R.; Tidwell,T.T.
Journal of the American Chemical Society, 1985 , vol. 107, p. 5391
