9-(4-溴-苯基)-10-苯基-蒽合成路线 （共 8 条）
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; water; toluene
T=90°C; 12 h;
参考文献
TDK Corporation
Patent: US2011/295017 A1, 2011 ;
Location in patent: Page/Page column 22-23 ;
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; toluene
T=110°C; 10 h;
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2008/81934 A1, 2008 ;
Location in patent: Page/Page column 36 ;
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran
T=80°C; 24 h; Inert atmosphere;
参考文献
Moorthy, Jarugu Narasimha; Venkatakrishnan, Parthasarathy; Natarajan, Palani; Huang, Duo-Fong; Chow, Tahsin J.
Journal of the American Chemical Society, 2008 , vol. 130, # 51 p. 17320 - 17333
参考文献
SEMICONDUCTOR ENERGY LABORATORY CO., LTD.
Patent: US2010/1638 A1, 2010 ;
反应条件
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / 120 °C
2.1: N-bromosuccinmide / dichloromethane / 24 h / 25 °C / Inert atmosphere
3.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere
3.2: 20 °C
4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 2 h / 120 °C
View Scheme
参考文献
Shin, Hyo Nim; Kim, Chi Sik; Kwon, Hyuck Joo; Cho, Young Jung; Kim, Bong Ok; Kim, Sung Min; Yoon, Seung Soo
Patent: US2011/152587 A1, 2011 ;
反应条件
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / 120 °C
2.1: N-bromosuccinmide / dichloromethane / 24 h / 25 °C / Inert atmosphere
3.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere
3.2: 20 °C
4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 2 h / 120 °C
View Scheme
参考文献
Shin, Hyo Nim; Kim, Chi Sik; Kwon, Hyuck Joo; Cho, Young Jung; Kim, Bong Ok; Kim, Sung Min; Yoon, Seung Soo
Patent: US2011/152587 A1, 2011 ;
反应条件
1.1: N-bromosuccinmide / dichloromethane / 24 h / 25 °C / Inert atmosphere
2.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere
2.2: 20 °C
3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 2 h / 120 °C
View Scheme
参考文献
Shin, Hyo Nim; Kim, Chi Sik; Kwon, Hyuck Joo; Cho, Young Jung; Kim, Bong Ok; Kim, Sung Min; Yoon, Seung Soo
Patent: US2011/152587 A1, 2011 ;
反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere
1.2: 20 °C
2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 2 h / 120 °C
View Scheme
参考文献
Shin, Hyo Nim; Kim, Chi Sik; Kwon, Hyuck Joo; Cho, Young Jung; Kim, Bong Ok; Kim, Sung Min; Yoon, Seung Soo
Patent: US2011/152587 A1, 2011 ;
