4-氯-alpha-环丙基-alpha-甲基苄醇合成路线 (共 4 条)
反应条件
1: p-Cl-C6H4-X With iodine; magnesium in diethyl ether
T=40 - 45°C; 2 h;
2: cyclopropane carboxylic acid cyanide in diethyl ether
T=20°C; 3 h;
参考文献
Singh, Chandan; Pandey, Shilpi; Saxena, Gunjan; Srivastava, Nisha; Sharma, Malvika
Journal of Organic Chemistry, 2006 , vol. 71, # 24 p. 9057 - 9061
反应条件
1: AlCl3
2: diethyl ether
View Scheme
参考文献
Sarel,S. et al.
Israel Journal of Chemistry, 1963 , vol. 1, p. 451 - 459
参考文献
Sarel,S. et al.
Israel Journal of Chemistry, 1963 , vol. 1, p. 451 - 459
反应条件
magnesium
1) ether, 20 deg C, 1 h, 2) ether, heating, 2 h; Yield given. Multistep reaction;
参考文献
Kostikov, R. R.; Molchanov, A. P.; Nagi, Sh. M.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1291 - 1297
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1437 - 1444