1: With dirhodium tetraacetate; hydrogen; triphenylphosphine in benzene T=80°C; P=20685.9 Torr; 20 h; 2: With lithium aluminium tetrahydride in benzene 2 h; Heating; Title compound not separated from byproducts;
参考文献
Bergmann, David J.; Campi, Eva M.; Roy Jackson; Patti, Antonio F.; Saylik, Dilek
Australian Journal of Chemistry, 2000 , vol. 53, # 10 p. 835 - 844
1: With hydrazine hydrate in ethanl
3 h; Reflux;
2: With hydrogenchloride in ethanol; water
pH=1 - 2;
3: With sodium hydroxide in ethanol; water
pH=10 - 11;