1: With tert.-butyl lithium in tetrahydrofuran; hexane
T=-78°C; 1 h; Inert atmosphere;
2: With tri-isopropoxy-borane in tetrahydrofuran; hexane
T=-78 - -30°C;
3: With potassium hydrogen difluoride in tetrahydrofuran; hexane
T=-30 - 20°C;
参考文献
Park, Young Hee; Ahn, Hong Ryul; Canturk, Belgin; Jeon, Sang Ii; Lee, Seokjoon; Kang, Heonjoong; Molander, Gary A.; Ham, Jungyeob
Organic Letters, 2008 , vol. 10, # 6 p. 1215 - 1218
