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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-碘苯酚
合成路线
（共 136 条）
626-02-8
3-碘苯酚
→
反应条件
143536-52-1
5-(3-羟基苯基)戊酸乙酯
反应条件
1.1: potassium carbonate; tetrabutyl-ammonium chloride / palladium diacetate / N,N-dimethyl-formamide / 1 h / 70 °C 1.2: 20 °C 2.1: hydrogen / palladium 10 on activated carbon / methanol / 2585.81 Torr View Scheme
参考文献
F. HOFFMANN-LA ROCHE AG; GILLESPIE, Paul; MICHOUD, Christophe; RUPERT, Kenneth Carey; THAKKAR, Kshitij Chhabilbhai; YI, Lin
Patent: WO2012/123467 A1, 2012 ;
292638-84-7
+
626-02-8
3-碘苯酚
→
反应条件
17861-18-6
反应条件
Pd(NH3)2Cl2; tributyl-amine; tetrabutylammomium bromide in water Heck Reaction; 24 h; Reflux;
参考文献
Marti-Centelles, Rosa; Cejudo-Marin, Rocio; Falomir, Eva; Murga, Juan; Carda, Miguel; Alberto Marco
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 11 p. 3010 - 3015
626-02-8
3-碘苯酚
→
反应条件
139102-37-7
反应条件
1: triethylamine; magnesium chloride / acetonitrile / 80 °C 2: potassium carbonate / N,N-dimethyl-formamide / 120 °C View Scheme
参考文献
Banerjee, Abhisek; Yadav, Pravin S.; Bajpai, Malini; Sangana, Ramachandra Rao; Gullapalli, Srinivas; Gudi, Girish S.; Gharat, Laxmikant A.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 9 p. 3223 - 3228
626-02-8
3-碘苯酚
→
反应条件
289039-26-5
2-氯-5-碘苯酚
反应条件
1: tetrachloromethane / 0 °C / Einleiten von Chlor 2: aqueous acetic acid; KI View Scheme
参考文献
Buchan; McCombie
Journal of the Chemical Society, 1932 , p. 2857,2860
626-02-8
3-碘苯酚
→
反应条件
22955-73-3
4-甲氧基间苯二甲酸二甲酯
反应条件
1: NaOH 2: Ag2O, aq. NaOH 3: aq. NaOH / Raney-Ni View Scheme
参考文献
Kobayashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1969 , vol. 17, p. 1279 - 1283
626-02-8
3-碘苯酚
→
反应条件
196597-26-9
雷美替胺
反应条件
1.1: potassium carbonate / acetone / 55 °C 2.1: AlCl3, aluminium chloride / dichloromethane / 2.5 h / 0 - 20 °C / |Inert atmosphere 3.1: norborn-2-ene; palladium diacetate; triphenylphosphine; caesium carbonate / 12 h / 80 °C 4.1: titanium tetraethoxide / tetrahydrofuran / 0.17 h / 0 °C / |Inert atmosphere 4.2: 24 h / 60 °C / |Inert atmosphere 5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / -78 °C / |Inert atmosphere; |Heating 6.1: hydrogenchloride; water / methanol / 4 h / 0 - 20 °C / |Inert atmosphere 7.1: palladium 10 on activated carbon; hydrogen / ethyl acetate; acetic acid / 24 h / 45 °C / 2068.65 Torr 8.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C / |Inert atmosphere 9.1: triethylamine / dichloromethane / 1 h / 20 °C 10.1: potassium phtalimide / N,N-dimethyl-formamide / 1 h / 100 °C 10.2: 3 h / |Reflux 11.1: triethylamine / dichloromethane / 20 °C View Scheme
参考文献
Fu, Xiaodan; Guo, Xingqun; Li, Xingwei; He, Lidong; Yang, Yushe; Chen, Youxi
Tetrahedron Asymmetry, 2013 , vol. 24, # 13-14 p. 827 - 832
626-02-8
3-碘苯酚
→
反应条件
214279-40-0
3-碘代-4-硝基茴香醚
反应条件
1: alcohol; diluted sulfuric acid; sodium nitrate / 15 °C 2: natrium carbonate View Scheme
参考文献
Hodgson; Moore
Journal of the Chemical Society, 1927 , p. 634
Journal of the Chemical Society, 1925 , vol. 127, p. 1602
626-02-8
3-碘苯酚
→
反应条件
191348-14-8
2-碘-4-甲氧基苯基胺
反应条件
1.1: aq. KOH; diazotized sulfanilic acid / 0.5 h 1.2: sodium hydrosulfite / H2O / 0.25 h / 45 °C 2.1: Cs2CO3 / dimethylformamide / 48 h / 20 °C View Scheme
参考文献
Jana, Goutam Kumar; Sinha, Surajit
Tetrahedron, 2012 , vol. 68, # 35 p. 7155 - 7165
626-02-8
3-碘苯酚
+
536-74-3
苯乙炔
→
反应条件
886-66-8
1,4-二苯基丁二炔
+
111731-38-5
1-苯基-2-(m-羟基苯基)乙炔
反应条件
triethylamine; palladium complex immobilised on silica gel in various solvent(s) T=70°C; Sonogashira coupling; 12 h;
参考文献
Bandini, Marco; Luque, Rafael; Budarin, Vitaly; Macquarrie, Duncan J.
Tetrahedron, 2005 , vol. 61, # 41 p. 9860 - 9868
626-02-8
3-碘苯酚
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
365426-93-3
反应条件
potassium carbonate; palladium 10 on activated carbon in water T=170°C; 0.333333 h; Microwave irradiation;
参考文献
BIOVITRUM AB (publ)
Patent: WO2008/743 A2, 2008 ;
Location in patent: Page/Page column 41 ;
WO 2008/000743 A2
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