反应条件
1: 1) n-BuLi / 1) Et2O, hexane, THF, -78 deg C, 2) THF, -78 deg C, 5 min
2: 1) NaH / 2) HMPA, r.t., 20 min
3: Mg-monoperoxyphthalate / methanol / 1 h / Ambient temperature
4: 1) n-BuLi / 1) Et2O, hexane, THF, -78 deg C, 2) THF, -78 deg C, 5 min
5: 1) n-BuLi / 1) Et2O-hexane-THF, -78 deg C, 5-10 min, 2) -78 deg C
View Scheme
参考文献
Uenishi, Jun'ichi; Tanaka, Takakazu; Nishiwaki, Kenji; Wakabayashi, Shoji; Oae, Shigeru; Tsukube, Hiroshi
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4382 - 4388
