n-butyllithium; iodine; diisopropylamine 1.) THF, hexane, -78 grad C, 30 min, 2.) THF, hexane, -78 grad C, then slowly allowed to warm to room temperature overnight.; Yield given. Multistep reaction;
参考文献
Gribble, Gordon W.,; Saulnier, Mark G.
Tetrahedron Letters, 1980 , vol. 21, p. 4137 - 4140
n-butyllithium; iodine; diisopropylamine 1.) THF, hexane, -78 grad C, 30 min, 2.) THF, hexane, -78 grad C, then slowly allowed to warm to room temperature overnight.; Yield given. Multistep reaction;
参考文献
Gribble, Gordon W.,; Saulnier, Mark G.
Tetrahedron Letters, 1980 , vol. 21, p. 4137 - 4140
