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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-氯吡啶
合成路线
（共 332 条）
626-60-8
3-氯吡啶
+
100-58-3
溴化苯基镁
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
CpPd(SIMes)Cl; lithium chloride in tetrahydrofuran; ethylene glycol dimethyl ether T=20°C; Kumada-Tamao-Corriu cross-coupling reaction; 36 h; Inert atmosphere;
参考文献
Iglesias, Maria Jose; Prieto, Auxiliadora; Nicasio, M. Carmen
Organic Letters, 2012 , vol. 14, # 17 p. 4318 - 4321
626-60-8
3-氯吡啶
+
71-43-2
苯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
HCN(CH2C(O)NHC6H5)CHCHN(CH2C6H5)(1+)*Cl(1-)=(HCN(CH2C(O)NHC6H5)CHCHN(CH2C6H5))Cl; potassium tert-butylate T=20 - 100°C; 20 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Ghosh, Debalina; Lee, Jhen-Yi; Liu, Chian-Yu; Chiang, Yen-Hsin; Lee, Hon Man
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 406 - 410
626-60-8
3-氯吡啶
+
934-56-5
三甲基(苯基)锡
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
α-cyclohexylcyclohexanemethanamine; [(t-Bu)2P(OH)]2PdCl2 in water T=140°C; Stille cross-coupling; 24 h;
参考文献
Wolf, Christian; Lerebours, Rachel
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7551 - 7554
626-60-8
3-氯吡啶
+
780-69-8
苯基三乙氧基硅烷
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); tetrabutylammomium bromide; sodium hydroxide in water T=60°C; Hiyama coupling; 8 h; Inert atmosphere;
参考文献
Lee, Dong-Hwan; Jung, Ji-Young; Jin, Myung-Jong
Chemical Communications, 2010 , vol. 46, # 47 p. 9046 - 9048
626-60-8
3-氯吡啶
+
143-66-8
四苯硼钠
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,3-bis-(diphenylphosphino)propane in xylene T=120°C; Suzuki-Miyaura cross-coupling; 20 h;
参考文献
Ueura, Kenji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2005 , vol. 7, # 11 p. 2229 - 2231
626-60-8
3-氯吡啶
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
tripotassium phosphate monohydrate; 1-methyl-2-(2-(dicyclohexylphosphino)phenyl)-1H-benzoimidazole; bis(dibenzylideneacetone)-palladium(0) in toluene; tert-butyl alcohol T=135°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Wong, Shun Man; So, Chau Ming; Chung, Kin Ho; Luk, Chi Him; Lau, Chak Po; Kwong, Fuk Yee
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3754 - 3757
626-60-8
3-氯吡啶
+
108-86-1
溴代苯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
bis(carbene)-derived nickel(II)-pincer complex in tetrahydrofuran T=20°C; Grignard coupling reaction; 48 h;
参考文献
Inamoto, Kiyofumi; Kuroda, Jun-Ichi; Sakamoto, Takao; Hiroya, Kou
Synthesis, 2007 , # 18 p. 2853 - 2861
626-60-8
3-氯吡啶
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [NiCl2(1,2-dimethoxyethane)]; caesium carbonate; zinc; tri-cyclo-hexyl-phosphine in N,N-dimethyl-formamide; acetone T=20 - 60°C; Suzuki-Miyaura cross-coupling reaction; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Chemical Communications, , vol. 47, # 1 p. 307 - 309
626-60-8
3-氯吡啶
+
4426-21-5
二苯基硼酸酐
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
triphenyl phosphite; K3PO4*3H2O; Ipr.HCl; palladium diacetate in tert-butyl alcohol T=80°C; 6 h; Inert atmosphere;
参考文献
Chen, Xiaofeng; Ke, Haihua; Chen, Yao; Guan, Changwei; Zou, Gang
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7572 - 7578
626-60-8
3-氯吡啶
+
368-47-8
苯基三氟硅烷
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
1: phenyl-trifluoro-silane With tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=20°C; Hiyama cross-coupling reaction; 0.0833333 h; Inert atmosphereSealed vial; 2: 3-chloro-pyridine in tert-butyl alcohol T=60°C; Hiyama cross-coupling reaction; Inert atmosphereSealed vial;
参考文献
Molander, Gary A.; Iannazzo, Laura
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9182 - 9187
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