反应条件
1.1: sulfuric acid; potassium nitrate / 1 h / 0 - 100 °C / |Inert atmosphere 2.1: trichlorophosphate / 1,2-dichloro-ethane / 4 h / 80 - 85 °C / |Inert atmosphere 2.2: 1 h / 0 - 65 °C / |Inert atmosphere 3.1: 100 °C / |Sealed tube; |Inert atmosphere 4.1: palladium on activated charcoal; hydrogen / ethanol; water / 4 h / 2585.81 Torr / |Inert atmosphere View Scheme
参考文献
Provencal, David P.; Gesenberg, Kirsten D.; Wang, Hua; Escobar, Carlos; Wong, Henry; Brown, Matthew A.; Staab, Andrew J.; Pendri, Yadagiri R.
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 903 - 908
