2-苯亚甲基-1-四氢萘酮合成路线 (共 24 条)
参考文献
Katritzky, Alan R.; Musumarra, Giuseppe; Sakizadeh, Kumars
Tetrahedron Letters, 1980 , vol. 21, p. 2701 - 2703
反应条件
palladium on activated charcoal T=240°C;
参考文献
Campbell et al.
Pr. roy. Soc. Edinburgh, 1957 , vol. <A> 65, p. 223,225
反应条件
aluminum oxide; potassium fluoride in N,N-dimethyl-formamide
T=80°C;
参考文献
Wang, Xiang-Shan; Zeng, Zhao-Sen; Shi, Da-Qing; Wei, Xian-Yong; Zong, Zhi-Min
Synthetic Communications, 2004 , vol. 34, # 18 p. 3265 - 3271
反应条件
bromine in tetrachloromethane
0.333333 h; Ambient temperature;
参考文献
Toth, Gabor,; Janke, Frank,; Levai, Albert
Liebigs Annalen der Chemie, 1989 , p. 651 - 654
反应条件
barium isopropoxide in N,N-dimethyl-formamide
T=20°C; 21 h;
参考文献
Yanagisawa, Akira; Takahashi, Hiroshi; Arai, Takayoshi
Tetrahedron, 2007 , vol. 63, # 35 p. 8581 - 8585
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane
8 h; Ambient temperature;
参考文献
Swamy, Vishwanath M.; Sarkar, Amitabha
Tetrahedron Letters, 1998 , vol. 39, # 10 p. 1261 - 1264
反应条件
1: 99 percent / Molecular sieves / toluene / 20 h / Heating
2: 75 percent / AcOH / H2O / 1.) reflux, 3 h, 2.) room temp., 12 h
View Scheme
参考文献
Katritzky, Alan R.; El-Mowafy, Azzahra M.; Musumarra, Giuseppe; Sakizadeh, Kumars; Sana-Ullah, Choudhry; et al.
Journal of Organic Chemistry, 1981 , vol. 46, # 19 p. 3823 - 3830
反应条件
1: 6 percent / P4S10, Et3N / CS2 / 2 h / 50 - 55 °C
2: 90 percent / benzene / 4 h / Heating
View Scheme
参考文献
Tanaka, Hideyuki; Kametani, Shunichi; Saito, Takao; Motoki, Shinichi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 2 p. 667 - 674
反应条件
1: 64 percent / 1.5 h / melt, then heating
2: 80 percent / 1.) acetic acid 2.) ammonium hydroxide / methanol / 5 h
View Scheme
参考文献
Katritzky, Alan R.; Brzezinski, Jacek Z.; Ou, Yu Xiang; Musumarra, Giuseppe
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1463 - 1470
反应条件
TMG
48 h; Ambient temperature;
参考文献
Black, David St. C.; Johnstone, Lynn M.
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 117 - 128