1,3,5-三苯基-1,5-戊二酮合成路线 (共 55 条)
反应条件
in tetrahydrofuran T=25°C;
参考文献
Katritzky, Alan R.; Harris, Philip A.
Tetrahedron, 1990 , vol. 46, # 3 p. 987 - 996
参考文献
Journal of the American Chemical Society, , vol. 41, p. 1263
反应条件
1: sodium ethylate; alcohol 2: zinc dust; alcohol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 41, p. 1263
反应条件
sodium ethanolate in neat (no solvent) T=80 - 85°C; Michael Addition; 0.0333333 h; Microwave irradiationGreen chemistry; Catalytic behavior; Reagent/catalystTime;
参考文献
Paul, Nidhin; Shanmugam, Muniyappapillai Jeganathan; Muthusubramanian, Shanmugam
Synthetic Communications, 2013 , vol. 43, # 1 p. 129 - 138
反应条件
in acetonitrile Addition; 2 h; Heating;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 36, # 5 p. 384 - 385
反应条件
1: MgCl2 / dimethylformamide / 24 h / 30 °C 2: aq. HCl / dimethylformamide / 0.08 h View Scheme
参考文献
Synlett, , # 13 p. 2068 - 2070
反应条件
1: MgCl2 / dimethylformamide / 24 h / 30 °C 2: aq. HCl / dimethylformamide / 0.08 h View Scheme
参考文献
Synlett, , # 13 p. 2068 - 2070
反应条件
1: 56 percent / NEt3 / CH2Cl2; petroleum ether / 1) -40 deg C, 60 min, 2) -40 deg C to RT, 60 min 2: 7 percent / 1) t-BuOK / multistep reaction; other ketones, other substrate View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 7 p. 1937 - 1942
反应条件
n-butyllithium; methylmesitylacetone; magnesium bromide in diethyl ether 17 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 40, # 20 p. 4127 - 4140
反应条件
n-butyllithium; magnesium bromide in diethyl ether 17 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 40, # 20 p. 4127 - 4140