四氢-alpha-[2-(四氢呋喃-2-基)乙基]-2-呋喃-1-丙醇合成路线 (共 12 条)
参考文献
Thomas
Bulletin de la Societe Chimique de France, 1954 , p. 529
反应条件
hydrogen; Al-Ni-Ti alloy in isopropyl alcohol
T=100°C; P=45600 Torr; 2 h;
参考文献
Mat'yakubov, R.; Mamatov, Yu. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 7 p. 651 - 655
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , # 7 p. 889 - 893
反应条件
1: furfural in water
T=49.84°C; Aldol condensation; P=7500.75 - 41254.1 Torr; 24 h; AutoclaveInert atmosphere;
2: acetone in water
Aldol condensation; 24 h; Inert atmosphere;
3: With hydrogen
T=119.84°C; P=33003.3 - 41254.1 Torr;
参考文献
Faba, Laura; Diaz, Eva; Ordonez, Salvador
Catalysis Today, 2011 , vol. 164, # 1 p. 451 - 456
反应条件
1: T=140°C; 5 h;
2: With hydrogen in isopropyl alcohol
T=140°C; P=30003 Torr; 10 h;
参考文献
Xu, Wenjie; Liu, Xiaohui; Ren, Jiawen; Zhang, Peng; Wang, Yanqin; Guo, Yanglong; Guo, Yun; Lu, Guanzhong
Catalysis Communications, 2010 , vol. 11, # 8 p. 721 - 726
反应条件
1: T=140°C; 5 h;
2: With hydrogen in isopropyl alcohol
T=120°C; P=30003 Torr; 10 h;
参考文献
Xu, Wenjie; Liu, Xiaohui; Ren, Jiawen; Zhang, Peng; Wang, Yanqin; Guo, Yanglong; Guo, Yun; Lu, Guanzhong
Catalysis Communications, 2010 , vol. 11, # 8 p. 721 - 726
反应条件
1: T=140°C; 5 h;
2: With hydrogen in isopropyl alcohol
T=80°C; P=30003 Torr; 10 h;
参考文献
Xu, Wenjie; Liu, Xiaohui; Ren, Jiawen; Zhang, Peng; Wang, Yanqin; Guo, Yanglong; Guo, Yun; Lu, Guanzhong
Catalysis Communications, 2010 , vol. 11, # 8 p. 721 - 726
反应条件
hydrogen; Al-Ni-Ti alloy in ethanol
T=50°C; P=760 Torr; 5 h; other solvents,other temperatures, other pressures; MechanismRate constantProduct distribution;
参考文献
Mat'yakubov, R.; Mamatov, Yu. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 7 p. 651 - 655
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , # 7 p. 889 - 893
反应条件
T=200°C; P=125036 - 147102 Torr; Hydrogenation;
参考文献
Alexander; Schniepp
Patent: US2657220 , 1951 ;
Full Text Show Details
Alexander; Schniepp
Patent: US2676972 , 1953 ;
Full Text Show Details
Russell et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4543,4545, 4546
反应条件
T=200°C; P=125036 - 147102 Torr; Hydrogenation;
参考文献
Alexander; Schniepp
Patent: US2657220 , 1951 ;
Full Text Show Details
Alexander; Schniepp
Patent: US2676972 , 1953 ;
Full Text Show Details
Russell et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4543,4545, 4546
反应条件
T=200°C; P=147102 Torr; Hydrogenation;
参考文献
Russell et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4543,4545, 4546