2-(4-氯苯基)苯并噻唑合成路线 （共 73 条）
反应条件
1: 72 percent / Et3N / diethyl ether / 12 h 2: 83 percent / tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 179, # 9 p. 1883 - 1891
反应条件
1: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C 2: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 16 p. 4840 - 4843
反应条件
1: phosphothion 2: Rb2CO3; tris-(dibenzylideneacetone)dipalladium(0); oxygen; tris-(o-tolyl)phosphine / water / 24 h / 40 °C / 760.05 Torr View Scheme
参考文献
Synlett, , vol. 23, # 11 p. 1678 - 1682
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux 2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C View Scheme
参考文献
Tetrahedron, , vol. 70, # 2 p. 245 - 250
反应条件
0.1 h; Microwave irradiationneat (no solvent);
参考文献
Dandia, Anshu; Singh, Ruby; Singh, Dharmendra; Laxkar, Ashok; Sivpuri, Asha
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 12 p. 2472 - 2479
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux 2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C View Scheme
参考文献
Tetrahedron, , vol. 70, # 2 p. 245 - 250
反应条件
1: Ambient temperature 2: triethylamine hydrochloride / 150 °C / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 5 p. 1780 - 1783
参考文献
Journal of Heterocyclic Chemistry, , vol. 16, p. 13 - 16
反应条件
t-Bu Brett Phos; C44H62NO5PPdS; sodium t-butanolate in 1,4-dioxane T=50°C; 20 h; Sealed tubeInert atmosphere;
参考文献
Organic Letters, , vol. 15, # 15 p. 3998 - 4001
反应条件
t-Bu Brett Phos; C44H62NO5PPdS; sodium t-butanolate in 1,4-dioxane T=20°C; 20 h; Sealed tubeInert atmosphere;
参考文献
Cheung, Chi Wai; Buchwald, Stephen L.
Organic Letters, 2013 , vol. 15, # 15 p. 3998 - 4001
