2-(苯基甲基)-苯并噻唑合成路线 （共 39 条）
反应条件
3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile
T=50°C; Barbier type reaction; 17 h;
参考文献
Begouin, Jeanne-Marie; Rivard, Michael; Gosmini, Corinne
Chemical Communications, 2010 , vol. 46, # 32 p. 5972 - 5974
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=55 - 60°C; Substitution; benzylation; 2.5 h;
参考文献
Angiolelli, Mary E.; Casalnuovo, Albert L.; Selby, Thomas P.
Synlett, 2000 , # 6 p. 905 - 907
反应条件
potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in dimethyl sulfoxide
T=120°C; 1 h; Inert atmosphere;
参考文献
Mukai, Tomoya; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2010 , vol. 12, # 6 p. 1360 - 1363
反应条件
caesium carbonate in 1,4-dioxane
T=115°C; 2 h;
参考文献
Feng, Enguang; Huang, He; Zhou, Yu; Ye, Deju; Jiang, Hualiang; Liu, Hong
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 4 p. 422 - 429
反应条件
1: 2-amino-benzenethiol With trimethylaluminum chloride in toluene
T=0 - 20°C;
2: hydroxymethyl JandaJelTM resin-bound benzyl ester in toluene
24 h; Heating; Further stages.;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,3,5-trimethyl-benzene
T=140°C; 10 h; Inert atmosphere;
参考文献
Shang, Rui; Yang, Zhi-Wei; Wang, Yan; Zhang, Song-Lin; Liu, Lei
Journal of the American Chemical Society, 2010 , vol. 132, # 41 p. 14391 - 14393
反应条件
in N,N-dimethyl-formamide
T=60°C; 2 h;
参考文献
Fan, Xuesen; He, Yan; Zhang, Xinying; Guo, Shenghai; Wang, Yangyang
Tetrahedron, 2011 , vol. 67, # 34 p. 6369 - 6374
反应条件
tri(n-propyl)amine; copper(l) iodide; 1,10-phenanthroline in 1,4-dioxane
T=20 - 100°C; Wittig Olefination; 32.0833 h; Inert atmosphere;
参考文献
Yu, Hui; Zhang, Meishu; Li, Yuzhe
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8898 - 8903
反应条件
iodine in 1,2-dichloro-ethane
T=80°C;
参考文献
Zhao, Dong-Yun; Guo, Xiao-Kang; Li, Jin-Heng; Tang, Ri-Yuan
Synthesis, 2012 , vol. 44, # 6 p. 927 - 933
反应条件
sodium dithionite in dimethyl sulfoxide
T=80°C; 10 h; Molecular sieve;
参考文献
Wang, Zhanglin; Tang, Riyuan; Xiao, Qin
Chinese Journal of Chemistry, 2011 , vol. 29, # 2 p. 314 - 320
