反-1,3-二苯基-2-丙稀-1-醇合成路线 （共 76 条）
反应条件
methyl-diethoxy-silane; ferrous acetate in tetrahydrofuran T=65°C;
参考文献
Tetrahedron Letters, , vol. 49, # 1 p. 110 - 113
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; Alkylation; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 40, # 40 p. 7159 - 7162
反应条件
1: 3-phenyl-3-hydroxypropene With α-cyclohexylcyclohexanemethanamine in water T=20°C; Heck reaction; 0.25 h; 2: iodobenzene With Kaiser oxime-derived complex on resin base in water T=120°C; Heck reaction; 16 h; Further stages. Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 17-18 p. 2572 - 2584
反应条件
[Rh(acac)2(CO)2] in tetrahydrofuran; water T=70°C; 15 h; Inert atmosphere;
参考文献
Jana, Ranjan; Tunge, Jon A.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8376 - 8385
反应条件
in toluene T=120°C; 16 h;
参考文献
Journal of Organometallic Chemistry, , vol. 241, # 1 p. 15 - 26
反应条件
1: MgSO4 / diethyl ether / 9 h / 20 °C 2: 85 percent / 1-phenylpropyne; H2O / Ni(cod)2 / dioxane / 12 h / 80 °C View Scheme
参考文献
Chemical Communications, , # 11 p. 1459 - 1461
反应条件
1: hexane / 20 °C 2: 21 percent / diethylzinc / toluene; hexane / 0.5 h / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 11 p. 3210 - 3211
反应条件
1: sodium hydroxide / methanol; water / 5 - 25 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 18 p. 5289 - 5291
反应条件
1: sodium hydroxide / methanol; water / 5 - 25 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 18 p. 5289 - 5291
反应条件
sodium tetrahydroborate; calcium trifluoromethane sulfonate in tetrahydrofuran; methanol T=20°C; 0.5 h; Inert atmosphere; regioselective reaction;
参考文献
Forkel, Nina V.; Henderson, David A.; Fuchter, Matthew J.
Green Chemistry, 2012 , vol. 14, # 8 p. 2129 - 2132
