反-1,3-二苯基-2-丙稀-1-醇合成路线 （共 76 条）
反应条件
1: DPP With N-bromosuccinmide; triphenylphosphine in tetrahydrofuran 0.25 h; 2: morpholine in tetrahydrofuran T=70°C; 2.5 h; Further stages.;
参考文献
Craig, Donald; King, N. Paul; Mountford, David M.
Chemical Communications, 2007 , # 10 p. 1077 - 1079
反应条件
[Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] in 1,2-dichloro-ethane T=80°C; 0.75 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 19 p. 3776 - 3785
反应条件
pyridine; oxygen; Pd(II)-hydrotalcite in toluene T=80°C; 3 h;
参考文献
Uemura; Kakiuchi; Nishimura; Inoue
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 1 p. 165 - 172
反应条件
manganese(IV) oxide; 1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine in acetonitrile T=20°C; 24 h;
参考文献
Synlett, , # 4 p. 521 - 524
反应条件
phenyllithium in tetrahydrofuran Isomerization; oxidation;
参考文献
Journal of Organic Chemistry, , vol. 63, # 17 p. 5730 - 5731
反应条件
potassium tert-butylate; [Ru(η5-Ph4MeCp)(CO)2Cl] in tetrahydrofuran; toluene T=20°C; 2.5 h;
参考文献
Martin-Matute, Belen; Bogar, Krisztian; Edin, Michaela; Kaynak, F. Betuel; Baeckvall, Jan-E.
Chemistry - A European Journal, 2005 , vol. 11, # 20 p. 5832 - 5842
反应条件
phenyllithium in tetrahydrofuran Isomerization; oxidation;
参考文献
Journal of Organic Chemistry, , vol. 63, # 17 p. 5730 - 5731
反应条件
1: HBr, FeCl3 / acetic acid 2: KOH View Scheme
参考文献
Staab,H.A.; Kurmeier,H.-A.
Chemische Berichte, 1968 , vol. 101, # 8 p. 2697 - 2708
反应条件
1: 78 percent / H2SO4 / 20 °C 2: Na / various solvent(s) View Scheme
参考文献
Doering; Birladeanu, Ludmila; Sarma, Keshab; Blaschke; Scheidemantel, Ursula; Boese; Benet-Bucholz, Jordi; Klaerner; Gehrke, Jan-Stephan; Zimny, Bernd Ulrich; Sustmann; Korth, Hans-Gert
Journal of the American Chemical Society, 2000 , vol. 122, # 2 p. 193 - 203
反应条件
1: pyridine; 4-dimethylaminopyridine / tetrahydrofuran / 20 °C 2: [(η3-allyl)Pd(S-BINAP(S))]SbF6 / ethyl acetate / 21 h / 20 °C View Scheme
参考文献
Faller; Wilt, Jeremy C.
Organic Letters, 2005 , vol. 7, # 4 p. 633 - 636
