9,10-二氢-9,9-二甲基吖啶合成路线 (共 15 条)
反应条件
1: With phosphoric acid T=20°C; 12 h; 2: With sodium hydroxide
参考文献
SOLVAY SA; BASCOUR, Dominique; MAUNOURY, Jonathan; ORSELLI, Enrico
Patent: WO2013/45411 A1, 2013 ;
Location in patent: Paragraph 00101 ;
反应条件
hydrogenchloride T=250°C;
参考文献
Journal of the American Chemical Society, , vol. 60, p. 1458,1464
反应条件
1: diethyl ether 2: 80 percent / H3PO4 / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 113, # 1 p. 358 - 384
反应条件
1: 66 percent / K2CO3 / Naturkupfer C / 170 - 180 °C 2: diethyl ether 3: 80 percent / H3PO4 / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 113, # 1 p. 358 - 384
反应条件
1: 66 percent / K2CO3 / Naturkupfer C / 170 - 180 °C 2: diethyl ether 3: 80 percent / H3PO4 / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 113, # 1 p. 358 - 384
反应条件
1: phosphoric acid / unter vermindertem Druck 2: concentrated aqueous hydrochloric acid / 250 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 60, p. 1458,1464
反应条件
1: potassium carbonate; copper (I)-iodide / 170 °C 2: phosphoric acid / unter vermindertem Druck 3: concentrated aqueous hydrochloric acid / 250 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 60, p. 1458,1464
反应条件
1: methyl magnesium iodide; dibutyl ether 2: dibutyl ether View Scheme
参考文献
Journal of the American Chemical Society, , vol. 58, p. 1278,1281
反应条件
anhydrous butyl ether
参考文献
Journal of the American Chemical Society, , vol. 58, p. 1278,1281
反应条件
methyl-magnesium iodide; anhydrous butyl ether
参考文献
Journal of the American Chemical Society, , vol. 58, p. 1278,1281