2-溴-5-甲氧基-1,3-二甲苯合成路线 （共 28 条）
反应条件
N-bromosuccinmide in acetonitrile T=20°C; Bromination; 12 h;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2605 - 2612
反应条件
potassium carbonate in acetone T=65°C; 8 h;
参考文献
Organic Letters, , vol. 7, # 17 p. 3721 - 3724
反应条件
potassium carbonate in acetone T=40°C; 17 h;
参考文献
Tetrahedron Letters, , vol. 51, # 42 p. 5546 - 5549
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane Bromination; 1 h; Heatingirradiation;
参考文献
Australian Journal of Chemistry, , vol. 52, # 11 p. 1093 - 1108
反应条件
bromine in acetic acid T=5°C; 4.5 h;
参考文献
Tetrahedron, , vol. 50, # 48 p. 13775 - 13800
反应条件
sodium hydroxide Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 116, # 3 p. 1016 - 1026
反应条件
1: 84 percent / KOH / methanol / 1 h / Heating 2: 85 percent / bromine / CCl4 / -5 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 10, # 16 p. 3931 - 3935
参考文献
Justus Liebigs Annalen der Chemie, , vol. 421, p. 57
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1.25 h; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane T=-78°C; 1.5 h;
参考文献
Moorthy, Jarugu Narasimha; Natarajan, Palani; Bajpai, Alankriti; Venugopalan, Paloth
Crystal Growth and Design, 2011 , vol. 11, # 8 p. 3406 - 3417
