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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6268-73-1
合成路线
（共 10 条）
1928-76-3
6-氯-9-(苯基甲基)-9H-嘌呤
→
反应条件
6268-73-1
反应条件
hydrazine hydrate in ethanol 3 h; Reflux;
参考文献
Chattopadhyay, Gautam; Ray, Parlha Sinha
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 4 p. 546 - 552
111267-84-6
→
反应条件
6268-73-1
反应条件
hydrazine hydrate in methanol 12 h; Ambient temperature;
参考文献
Hosmane, Ramachandra S.; Lim, Benjamin B.; Burnett, Friedrich N.
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 382 - 386
111267-86-8
→
反应条件
6268-73-1
反应条件
1: 47 percent / trifluoroacetic acid / toluene; methanol / 72 h / Heating 2: 84 percent / trifluoroacetic acid / 4 h / Heating 3: 81 percent / hydrazine monohydrate / methanol / 12 h / Ambient temperature View Scheme
参考文献
Hosmane, Ramachandra S.; Lim, Benjamin B.; Burnett, Friedrich N.
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 382 - 386
100-46-9
苄胺
→
反应条件
6268-73-1
反应条件
1: 88 percent / acetonitrile / 12 h / Ambient temperature 2: 84 percent / trifluoroacetic acid / 4 h / Heating 3: 81 percent / hydrazine monohydrate / methanol / 12 h / Ambient temperature View Scheme
参考文献
Hosmane, Ramachandra S.; Lim, Benjamin B.; Burnett, Friedrich N.
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 382 - 386
60598-48-3
5-氨基-1-苄基-1H-咪唑-4-甲腈
→
反应条件
6268-73-1
反应条件
1: 84 percent / trifluoroacetic acid / 4 h / Heating 2: 81 percent / hydrazine monohydrate / methanol / 12 h / Ambient temperature View Scheme
参考文献
Hosmane, Ramachandra S.; Lim, Benjamin B.; Burnett, Friedrich N.
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 382 - 386
3815-69-8
→
反应条件
6268-73-1
反应条件
1: 2 h / 180 °C 2: thionyl chloride / N,N-dimethyl-formamide / 1 h / |Heating 3: hydrazine hydrate / ethanol / 3 h / |Reflux View Scheme
参考文献
Chattopadhyay, Gautam; Ray, Parlha Sinha
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 4 p. 546 - 552
14013-11-7
9-苄基肌苷
→
反应条件
6268-73-1
反应条件
1: thionyl chloride / N,N-dimethyl-formamide / 1 h / |Heating 2: hydrazine hydrate / ethanol / 3 h / |Reflux View Scheme
参考文献
Chattopadhyay, Gautam; Ray, Parlha Sinha
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 4 p. 546 - 552
6268-73-1
→
反应条件
25491-56-9
反应条件
water; oxygen; copper(II) sulfate T=80°C; 6 h; Green chemistry; Catalytic behavior; Reagent/catalystConcentrationTemperatureTime;
参考文献
Xia, Ran; Xie, Ming-Sheng; Niu, Hong-Ying; Qu, Gui-Rong; Guo, Hai-Ming
Green Chemistry, 2014 , vol. 16, # 3 p. 1077 - 1081
6268-73-1
→
反应条件
25491-56-9
反应条件
water; water-d2; oxygen; copper(II) sulfate T=80°C; 6 h; Green chemistry;
参考文献
Xia, Ran; Xie, Ming-Sheng; Niu, Hong-Ying; Qu, Gui-Rong; Guo, Hai-Ming
Green Chemistry, 2014 , vol. 16, # 3 p. 1077 - 1081
122-51-0
原甲酸三乙酯
+
6268-73-1
→
反应条件
4022-95-1
反应条件
in N,N-dimethyl-formamide T=125 - 130°C; 2 h;
参考文献
Chattopadhyay, Gautam; Ray, Parlha Sinha
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 4 p. 546 - 552
