2-(2-氯苯基)-1,3-苯并噻唑合成路线 （共 19 条）
反应条件
diethyl phosphorobromidate in acetonitrile
T=20°C; 4 h;
参考文献
Patil, Sachin S.; Bobade, Vivek D.
Synthetic Communications, 2010 , vol. 40, # 2 p. 206 - 212
反应条件
in N,N-dimethyl-formamide
T=130 - 140°C;
参考文献
Shirinian; Melkova; Belen'kii; Krayushkin
Russian Chemical Bulletin, 2000 , vol. 49, # 11 p. 1859 - 1862
反应条件
D-glucopyranose; oxygen; glucose oxidase; chloroperoxidase
pH=6; 12 h; Citrate bufferEnzymatic reaction;
参考文献
Kumar, Atul; Sharma, Siddharth; Maurya, Ram Awatar
Tetrahedron Letters, 2010 , vol. 51, # 48 p. 6224 - 6226
反应条件
1: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C
2: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C
View Scheme
参考文献
Deng, Hang; Li, Zhengkai; Ke, Fang; Zhou, Xiangge
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4840 - 4843
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux
2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C
View Scheme
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
sodium hydride
1.) THF, RT, 15 min, 2.) THF, 60 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Mettey, Yvette; Michaud, Sabine; Vierfond, Jean Michel
Heterocycles, 1994 , vol. 38, # 5 p. 1001 - 1006
反应条件
1: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
View Scheme
参考文献
Lin, Yu-Chin; Li, Ni-Ching; Cherng, Yie-Jia
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 3 p. 808 - 814
反应条件
1: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
View Scheme
参考文献
Lin, Yu-Chin; Li, Ni-Ching; Cherng, Yie-Jia
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 3 p. 808 - 814
参考文献
Deshpande et al.
Journal of Scientific and Industrial Research, 1957 , vol. 16 B, p. 136
