反应条件
1: 1.) diisobutylalane, 2.) Pd(PPh3)4 / 1.) hexane, 20 deg C - 0.5 h, 50 deg C - 5 h, 2.) hexane, THF, 20 deg C, 0.5 h, reflux - 0.5 h 2: 1.) diisobutylalane, 2.) aq. potassium sodium tartrate / 1.) hexane, CH2Cl2, -78 deg C, 5 h, 2.) hexane, CH2Cl2, methanol View Scheme
参考文献
Bellina, Fabio; Carpita, Adriano; Corradi, Chiara; Rossi, Renzo
Synthetic Communications, 1996 , vol. 26, # 17 p. 3297 - 3316
