1-苯基-1,2-乙二醇二乙酸盐合成路线 (共 74 条)
反应条件
DBN in acetonitrile
T=80°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Taylor, James E.; Williams, Jonathan M.J.; Bull, Steven D.
Tetrahedron Letters, 2012 , vol. 53, # 32 p. 4074 - 4076
反应条件
sodium acetate; copper diacetate; Manganese (II) acetate in acetic anhydride; acetic acid
T=95 - 97°C; anodic oxidation;
参考文献
Shundo, Ryushi; Nishiguchi, Ikuzo; Matsubara, Yoshiharu; Hirashima, Tsuneaki
Tetrahedron, 1991 , vol. 47, # 4/5 p. 831 - 840
反应条件
indium(III) perchlorate; lithium perchlorate in ethyl acetate
T=20°C; 24 h;
参考文献
Chapman, Christopher J.; Frost, Christopher G.; Hartley, Joseph P.; Whittle, Alan J.
Tetrahedron Letters, 2001 , vol. 42, # 5 p. 773 - 775
反应条件
dihydrogen peroxide; ruthenium trichloride in acetic acid
T=80°C;
参考文献
Barak, Gabriela; Sasson, Yoel
Journal of the Chemical Society, Chemical Communications, 1987 , # 16 p. 1266 - 1267
反应条件
iron(III) chloride
T=0°C; 0.25 h;
参考文献
Corey, E. J.; Eckrich, Thomas M.
Tetrahedron Letters, 1983 , vol. 24, # 31 p. 3165 - 3168
反应条件
sodium acetate in acetic acid
T=70°C; Oxidation; 15 h; Electrolysis;
参考文献
Dubey, Shipra; Singh, Dan; Misra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999 , vol. 38, # 5 p. 548 - 552
反应条件
trifluorormethanesulfonic acid in acetic acid
T=20°C; Cooling with ice;
参考文献
Kang, Yan-Biao; Gade, Lutz H.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1610 - 1615
反应条件
copper(II) bis(trifluoromethanesulfonate) in dichloromethane
T=40°C; 16 h;
参考文献
Seayad, Jayasree; Seayad, Abdul Majeed; Chai, Christina L. L.
Organic Letters, 2010 , vol. 12, # 7 p. 1412 - 1415
反应条件
cesium fluoride in acetonitrile
1 h;
参考文献
Kunieda, Takehisa; Higuchi, Tsunehiko; Abe, Yoshihiro; Hirobe, Masaaki
Tetrahedron, 1983 , vol. 39, # 20 p. 3253 - 3260
反应条件
cesium fluoride in acetonitrile
8 h; Ambient temperatureother catalists: tertiery amine, Lewis acids;
参考文献
Kunieda, Takehisa; Higuchi, Tsunehiko; Abe, Yoshihiro; Hirobe, Masaaki
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1159 - 1160