(9ci)-2-(2-丙烯基)-苯甲醛合成路线 （共 27 条）
反应条件
bis(1,5-cyclooctadiene)nickel (0); It-Bu2 in 1,3,5-trimethyl-benzene T=130°C; 5 h; Inert atmosphere; Reagent/catalystSolvent;
参考文献
Hoshimoto, Yoichi; Hayashi, Yukari; Suzuki, Haruka; Ohashi, Masato; Ogoshi, Sensuke
Angewandte Chemie - International Edition, 2012 , vol. 51, # 43 p. 10812 - 10815
Angew. Chem., 2012 , vol. 124, # 43 p. 10970 - 10973,4
反应条件
bis(1,5-cyclooctadiene)nickel (0); C{N(2,6-iPr2C6H3)CH}2 in toluene T=130°C; 24 h; Inert atmosphere; Reagent/catalyst;
参考文献
Hoshimoto, Yoichi; Hayashi, Yukari; Suzuki, Haruka; Ohashi, Masato; Ogoshi, Sensuke
Angewandte Chemie - International Edition, 2012 , vol. 51, # 43 p. 10812 - 10815
Angew. Chem., 2012 , vol. 124, # 43 p. 10970 - 10973,4
反应条件
lt;RhCl(PPh)2gt;2 in dichloromethane T=40°C; 43 h; MechanismProduct distribution;
参考文献
Kampmeier, J. A.; Harris, S. H.; Mergelsberg, I
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 621 - 625
反应条件
lt;RhCl(PPh)2gt;2 in dichloromethane T=40°C; 43 h; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 4 p. 621 - 625
反应条件
lt;RhCl(PPh)2gt;2 in dichloromethane T=40°C; 43 h; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 4 p. 621 - 625
反应条件
FeCl3·6H2O in dichloromethane
参考文献
Lin, Song; Song, Chun-Xiao; Cai, Gui-Xin; Wang, Wen-Hua; Shi, Zhang-Jie
Journal of the American Chemical Society, 2008 , vol. 130, p. 12901 - 12903
反应条件
1: 1-bromo-2-(prop-2-enyl)benzene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; Inert atmosphere;
2: N,N-dimethyl-formamide in tetrahydrofuran; hexane
T=-78 - 20°C; Inert atmosphere;
参考文献
Watson, Iain D. G.; Ritter, Stefanie; Toste, F. Dean
Journal of the American Chemical Society, 2009 , vol. 131, p. 2056 - 2057
反应条件
pyridinium chlorochromate in dichloromethane
T=25°C; 0.5 h;
参考文献
Semmelhack,M.F.; Zask,A.
Journal of the American Chemical Society, 1983 , vol. 105, p. 2034
反应条件
1: 2-Iodobenzaldehyde With lithium dineopentylcuprate in tetrahydrofuran
T=-40 - -20°C; 4 h;
2: allyl bromide in tetrahydrofuran
T=20°C;
参考文献
Piazza, Claudia; Knochel, Paul
Angewandte Chemie - International Edition, 2002 , vol. 41, # 17 p. 3263 - 3265
反应条件
1: (2-iodophenyl)trimethylsilanyloxyacetonitrile With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran
T=-78°C; 0.5 h;
2: allyl bromide in tetrahydrofuran
T=-78 - 20°C;
3: With sodium hydroxide; copper(II) sulfate in ethanol
T=20°C; 2 h;
参考文献
Liu, Ching-Yuan; Ren, Hongjun; Knochel, Paul
Organic Letters, 2006 , vol. 8, # 4 p. 617 - 619
