4A,5,8,8a-四氢-[1,4]萘醌合成路线 （共 15 条）
反应条件
1: 91 percent / AcOH; aq. HBr / 0.25 h / 110 - 115 °C 2: 68 percent / NaOH / H2O / 12 h / 20 °C 3: 91 percent / m-CPBA / CH2Cl2 / 12 h / 20 °C 4: 42 percent / MgBr2*Et2O / toluene / 6 h / Heating View Scheme
参考文献
Tririya, Gasirat; Zanger, Murray
Synthetic Communications, 2004 , vol. 34, # 17 p. 3047 - 3059
参考文献
Halton, Brian; Kay, Andrew J.; Zhi-mei, Zha; Boese, Roland; Haumann, Thomas
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 12 p. 1445 - 1452
反应条件
1: 91 percent / AcOH; aq. HBr / 0.25 h / 110 - 115 °C 2: 68 percent / NaOH / H2O / 12 h / 20 °C View Scheme
参考文献
Halton, Brian; Stang, Peter J.
Synlett, 1997 , vol. 1997, # 2 p. 145 - 158
反应条件
H7PMo8V4O40 T=70°C; 1 h;
参考文献
Zhizhina; Simonova; Russkikh; Matveev
Russian Journal of Applied Chemistry, 2005 , vol. 78, # 5 p. 758 - 764
反应条件
hydrogen bromide; acetic acid T=110 - 115°C; 0.25 h;
参考文献
Tririya, Gasirat; Zanger, Murray
Synthetic Communications, 2004 , vol. 34, # 17 p. 3047 - 3059
反应条件
in benzene
T=40°C; 120 h;
参考文献
Halton, Brian; Kay, Andrew J.; Zhi-mei, Zha; Boese, Roland; Haumann, Thomas
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 12 p. 1445 - 1452
参考文献
Diels; Alder
Chemische Berichte, 1929 , vol. 62, p. 2357
参考文献
Diels; Alder
Chemische Berichte, 1929 , vol. 62, p. 2357
反应条件
1: 91 percent / AcOH; aq. HBr / 0.25 h / 110 - 115 °C
2: 68 percent / NaOH / H2O / 12 h / 20 °C
3: 91 percent / m-CPBA / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Tririya, Gasirat; Zanger, Murray
Synthetic Communications, 2004 , vol. 34, # 17 p. 3047 - 3059
反应条件
potassium hydroxide in acetone
4.5 h;
参考文献
Suzuki; Kimura; Terashima
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 11 p. 3559 - 3572
