2,2'-亚甲基二[5-(二乙基氨基)苯酚]合成路线 （共 4 条）
反应条件
1: With sulfuric acid in water T=140°C; Inert atmosphere; 2: With sodium hydroxide in water T=5 - 20°C; pH=9; 3: With hydrogenchloride; sodium nitrite in water T=20°C;
参考文献
WISTA LABORATORIES LTD.; CLUNAS, Scott; STRORY, John, Mervyn, David; RICKARD, Janet, Elizabeth; HORSLEY, David; HARRINGTON, Charles, Robert; WISCHIK, Claude, Michel
Patent: WO2010/67078 A2, 2010 ;
Location in patent: Page/Page column 65 ;
反应条件
1: With hydrogenchloride in water; isopropyl alcohol
T=20°C; 3.66667 h;
2: With ammonium hydrogen carbonate in water; isopropyl alcohol
1.58333 h;
参考文献
WISTA LABORATORIES LTD.; CLUNAS, Scott; STRORY, John, Mervyn, David; RICKARD, Janet, Elizabeth; HORSLEY, David; HARRINGTON, Charles, Robert; WISCHIK, Claude, Michel
Patent: WO2010/67078 A2, 2010 ;
Location in patent: Page/Page column 64, 65 ;
反应条件
hydrogenchloride; sodium acetate
参考文献
Biehringer
Journal fuer Praktische Chemie (Leipzig), 1896 , vol. <2> 54, p. 235
Full Text Show Details
Leonhardt and Co.
Patent: DE63081 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 93
Full Text Show Details
Leonhardt and Co.
Patent: DE58955 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 92
参考文献
Biehringer
Journal fuer Praktische Chemie (Leipzig), 1896 , vol. <2> 54, p. 235
Full Text Show Details
Leonhardt and Co.
Patent: DE58995 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 92,93
Full Text Show Details
Leonhardt and Co.
Patent: DE63081 ;
