5-甲酰胺[3,4'-联吡啶]-6(1H)-酮合成路线 （共 7 条）
反应条件
sodium hypochlorite; sodium sulfite in sodium hydroxide 1) 30 deg C, 15 min; 40 deg C, 15 min, 2) 40 deg C, 20 min;
参考文献
Niedrich; Heyne; Schrotter; et al.
Pharmazie, 1986 , vol. 41, # 3 p. 173 - 175
反应条件
potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate in acetonitrile
20 h; Heating;
参考文献
Gomez-Parra; Gonzalez; Sanchez; Torres
Archiv der Pharmazie, 1984 , vol. 317, # 2 p. 183 - 185
反应条件
sulfuric acid; potassium hydrogencarbonate
参考文献
Sterling Drug Inc.
Patent: US4004012 A1, 1977 ;
反应条件
sodium methylate in N-methyl-acetamide; methanol; water
参考文献
Sterling Drug Inc.
Patent: US4107315 A1, 1978 ;
反应条件
sodium hydroxide in water
T=60°C; 3 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Niedrich; Heyne; Schrotter; et al.
Pharmazie, 1986 , vol. 41, # 3 p. 173 - 175
反应条件
sulfuric acid
T=80°C; 2 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Niedrich; Heyne; Schrotter; et al.
Pharmazie, 1986 , vol. 41, # 3 p. 173 - 175
反应条件
in N-methyl-acetamide; water; mineral oil
参考文献
Sterling Drug Inc.
Patent: US4264609 A1, 1981 ;
