反应条件
1: bis(trichloromethyl) carbonate; N-Boc-2,2'-(ethylene-1,2-dioxy)bisethylamine With N-ethyl-N,N-diisopropylamine in dichloromethane
T=15 - 20°C; 1 h;
2: carbonic acid bis-(4-formyl-2,6-dimethyl-phenyl) ester With 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=20°C;
参考文献
Greenwald, Richard B.; Zhao, Hong; Xia, Jing; Martinez, Anthony
Journal of Medicinal Chemistry, 2003 , vol. 46, # 23 p. 5021 - 5030