螺[2H-1-苯并吡喃-2,1-环戊并n]-4(3h)-酮合成路线 (共 7 条)
反应条件
1: 92 percent / thallium(III) p-tosylate / acetonitrile / 1 h / Heating 2: 80 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / dioxane / 18 h / Heating View Scheme
参考文献
Singh, Om V.; George, Varughese; Kapil, Randhir S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 10 p. 856 - 864
参考文献
Kabbe, Hans-Joachim; Widdig, Arno
Angewandte Chemie, 1982 , vol. 94, # 4 p. 254 - 262
反应条件
sodium hydroxide in water; toluene
参考文献
Bayer Aktiengesellschaft
Patent: US4415741 A1, 1983 ;
参考文献
Bayer Aktiengesellschaft
Patent: US4185112 A1, 1980 ;
反应条件
pyrrolidine in toluene
1.) RT, 1 h, 2.) reflux, 8 h;
参考文献
Singh, Om V.; George, Varughese; Kapil, Randhir S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 10 p. 856 - 864
反应条件
pyrrolidine in toluene
Heating;
参考文献
Kabbe, Hans-Joachim; Widdig, Arno
Angewandte Chemie, 1982 , vol. 94, # 4 p. 254 - 262
反应条件
sodium tetrahydroborate in methanol
24 h;
参考文献
Brogden, Peter J.; Hepworth, John D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 827 - 830