1-碘基-3,5-二硝基苯合成路线 （共 23 条）
反应条件
copper(l) iodide; sodium iodide; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane T=110°C; 31 h;
参考文献
Jian, Huahua; Tour, James M.
Journal of Organic Chemistry, 2005 , vol. 70, # 9 p. 3396 - 3424
反应条件
TICA T=70°C; 17 h; Darkness; regioselective reaction;
参考文献
Da Ribeiro, Rodrigo S.; Esteves, Pierre M.; De Mattos, Marcio C. S.
Synthesis, 2011 , # 5 p. 739 - 744
反应条件
1: With sulfuric acid; silica gel; sodium nitrite T=20°C; grindingNeat (no solvent); 2: With water T=20°C; grindingNeat (no solvent); 3: With potassium iodide T=20°C; Sandmeyer reaction; 0.166667 h; grindingNeat (no solvent);
参考文献
Zarei, Amin; Hajipour, Abdol R.; Khazdoozd, Leila
Synthesis, 2009 , # 6 art. no. Z19108SS, p. 941 - 944
反应条件
iodine in Petroleum ether
参考文献
US5089513 A1, ;
US 5089513 A
反应条件
tert.-butylnitrite in acetonitrile T=22°C; 1 h;
参考文献
Ek, Fredrik; Wistrand, Lars-Goeran; Frejd, Torbjoern
Journal of Organic Chemistry, 2003 , vol. 68, # 5 p. 1911 - 1918
反应条件
potassium iodide in acetonitrile 1 h;
参考文献
Kosynkin, Dmitry; Bockman, T. Michael; Kochi, Jay K.
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 10 p. 2003 - 2012
反应条件
in water T=100.4°C; ΔH(excit.), ΔS(excit.); other temp.; Rate constantThermodynamic dataKinetics;
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 1041 - 1045
反应条件
in water T=125.6°C; ΔH(excit.), ΔS(excit.); other temp.; Rate constantThermodynamic dataKinetics;
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 1041 - 1045
反应条件
1: S, aq. Na2S 2: NaNO2, aq. HBF4 3: (pyrolysis) View Scheme
参考文献
Fletcher,T.L. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 1342 - 1348
反应条件
sodium acetate; palladium diacetate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=90°C; Heck reaction; P=7600.51 Torr; 0.5 h; Inert atmosphereAutoclave;
参考文献
Applied Organometallic Chemistry, , vol. 25, # 4 p. 289 - 293
